Information Package / Course Catalogue - Adnan Menderes University

General Information Unit Staff Academic Information Programme Outcomes Course Structure Diagram Contact Information

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Sample Preparation For Analysis

Course Code	: KİM515
Course Type	: Area Elective
Couse Group	: Second Cycle (Master's Degree)
Education Language	: Turkish
Work Placement	: N/A

Theory	: 3
Prt.	: 0
Credit	: 3
Lab	: 0
ECTS	: 6

Objectives of the Course

According to applied instrumental method, giving basic information about samples preparation for analysis such as solid, liquid, gas different physical states

Course Content

Techniques used in sample pre-treatment. Especially solid-liquid, liquid-liquid extraction techniques. Microwave extraction and supercritical fluid extraction techniques.

Name of Lecturer(s)

Learning Outcomes

1.	to be able to recognize the methods of sample preparation
2.	to be able to recognize the methods of sample analysis
3.	Learning the preconcentration techniques.
4.	Learning the extraction techniques.
5.	To learn sample preparation techniques for chromatographic analysis.

Recommended or Required Reading

1.	Mitra S. (2003), Sample preparation techniques in analytical chemistry, Wiley & Sons Publication
2.	Dean J. R. (2003), Methods for environmental trace analysis, John Wiled Sons Ltd.
3.	Sample preparation in chromatography, Journal of chromatography library, Volume:65

Weekly Detailed Course Contents

Week 1 - Theoretical

Extraction and basics of enrichment for sample preparation

Week 2 - Theoretical

Basics of extraction and Extraction of semi-volatile organic compounds from liquids

Week 3 - Theoretical

Liquid-liquid extraction, liquid-solid extraction

Week 4 - Theoretical

Solid-phase extraction, solid-phase microextraction

Week 5 - Theoretical

Extraction of semi-volatile organic compounds from solid matrices

Week 6 - Theoretical

Soxhlet extraction, ultrasonic extraction

Week 7 - Theoretical

Supercritical fluid extraction, microwave-assisted extraction

Week 8 - Intermediate Exam

Midterm Exam

Week 9 - Theoretical

Extraction of volatile organic compounds from solids and liquids

Week 10 - Theoretical

Preparation of samples for metal analysis

Week 11 - Theoretical

Microwave extraction for metal analysis

Week 12 - Theoretical

Organic extraction of metals, extraction with the supercritical fluid for metal analysis

Week 13 - Theoretical

Ultrasonic sample preparation, solid-phase extraction for preconcentration

Week 14 - Theoretical

Student Presentations

Assessment Methods and Criteria

Type of Assessment	Count	Percent
Assignment	3	%20
Midterm Examination	1	%10
Final Examination	1	%70

Workload Calculation

Activities	Count	Preparation	Time	Total Work Load (hours)
Lecture - Theory	14	0	3	42
Assignment	1	28	2	30
Midterm Examination	1	34	2	36
Final Examination	1	40	2	42
TOTAL WORKLOAD (hours)				150

Contribution of Learning Outcomes to Programme Outcomes

	PÇ-1	PÇ-2	PÇ-3	PÇ-4	PÇ-5	PÇ-6	PÇ-7	PÇ-8	PÇ-9
OÇ-1	4	4	4	4	4
OÇ-2	5	5	5	5	5
OÇ-3	4	4	4	4	4
OÇ-4	4	4	4	4	4
OÇ-5	4	4	4	4	4

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