Information Package / Course Catalogue
Sample Preparation For Analysis
Course Code: KİM515
Course Type: Area Elective
Couse Group: Second Cycle (Master's Degree)
Education Language: Turkish
Work Placement: N/A
Theory: 3
Prt.: 0
Credit: 3
Lab: 0
ECTS: 8
Objectives of the Course

According to applied instrumental method, giving basic information about samples preparation for analysis such as solid, liquid, gas different physical states

Course Content

Techniques used in sample pre-treatment. Especially solid-liquid, liquid-liquid extraction techniques. Microwave extraction and supercritical fluid extraction techniques.

Name of Lecturer(s)
Learning Outcomes
1.to be able to recognize the methods of sample preparation
2.to be able to recognize the methods of sample analysis
3.Learning the preconcentration techniques.  
4.Learning the extraction techniques.  
5.To learn sample preparation techniques for chromatographic analysis.
Recommended or Required Reading
1.Mitra S. (2003), Sample preparation techniques in analytical chemistry, Wiley & Sons Publication
2.Dean J. R. (2003), Methods for environmental trace analysis, John Wiled Sons Ltd.
3.Sample preparation in chromatography, Journal of chromatography library, Volume:65
Weekly Detailed Course Contents
Week 1 - Theoretical
Extraction and basics of enrichment for sample preparation
Week 2 - Theoretical
Basics of extraction and Extraction of semi-volatile organic compounds from liquids
Week 3 - Theoretical
Liquid-liquid extraction, liquid-solid extraction
Week 4 - Theoretical
Solid-phase extraction, solid-phase microextraction
Week 5 - Theoretical
Extraction of semi-volatile organic compounds from solid matrices
Week 6 - Theoretical
Soxhlet extraction, ultrasonic extraction
Week 7 - Theoretical
Supercritical fluid extraction, microwave-assisted extraction
Week 8 - Intermediate Exam
Midterm Exam
Week 9 - Theoretical
Extraction of volatile organic compounds from solids and liquids
Week 10 - Theoretical
Preparation of samples for metal analysis
Week 11 - Theoretical
Microwave extraction for metal analysis
Week 12 - Theoretical
Organic extraction of metals, extraction with the supercritical fluid for metal analysis
Week 13 - Theoretical
Ultrasonic sample preparation, solid-phase extraction for preconcentration
Week 14 - Theoretical
Student Presentations
Assessment Methods and Criteria
Type of AssessmentCountPercent
Assignment3%20
Midterm Examination1%10
Final Examination1%70
Workload Calculation
ActivitiesCountPreparationTimeTotal Work Load (hours)
Lecture - Theory140342
Assignment120020
Midterm Examination116218
Final Examination116218
TOTAL WORKLOAD (hours)98
Contribution of Learning Outcomes to Programme Outcomes
PÇ-1
PÇ-2
PÇ-3
PÇ-4
PÇ-5
OÇ-1
OÇ-2
OÇ-3
3
OÇ-4
OÇ-5
Adnan Menderes University - Information Package / Course Catalogue
2026